High resolution NMR : theory and chemical applications /
Saved in:
Main Authors: | |
---|---|
Corporate Authors: | |
Published: |
Academic Press,
|
Publisher Address: | New York : |
Publication Dates: | 1980. |
Literature type: | eBook |
Language: | English |
Edition: | 2d edition. |
Subjects: | |
Online Access: |
http://www.sciencedirect.com/science/book/9780120846603 |
Carrier Form: | 1 online resource (xiv, 354 pages) : illustrations |
Bibliography: | Includes bibliographical references and index. |
ISBN: |
9780323161855 0323161855 9781483293691 1483293696 |
Index Number: | QD96 |
CLC: | O657.2 |
Contents: |
Origins and Early History of NMR -- High Resolution NMR: An Overview -- The Theory of NMR -- Nuclear Spin and Magnetic Moment -- Theoretical Descriptions of NMR -- Steady-State Quantum Mechanical Description -- Effect of the Boltzmann Distribution -- Spin-Lattice Relaxation -- Precession of Nuclear Magnetic Moments -- Classical Mechanical Description of NMR -- Magnetization in the Rotating Frame -- Methods of Obtaining NMR Spectra -- Dynamic Processes -- Terminology, Symbols, Units, and Conventions -- Instrumentation and Techniques -- Advantages of Pulse Fourier Transform NMR -- Basic NMR Apparatus -- Requirements for High Resolution NMR -- Detection of NMR Signals -- Phase Cycling -- Fourier Transformation of the FID -- Data Acquisition -- Data Processing -- Digital Filtering -- Alternatives to Fourier Transformation -- Sensitivity and Size of Sample -- Useful Solvents -- Chemical Shifts -- The Origin of Chemical Shifts -- Theory of Chemical Shifts -- Measurement of Chemical Shifts -- Empirical Correlations of Chemical Shifts -- Some Aspects of Proton Chemical Shifts -- Nuclei Other Than Hydrogen -- Compilations of Spectral Data and Empirical Estimates of Chemical Shifts -- Isotope Effects -- Effects of Molecular Asymmetry -- Paramagnetic Species -- Coupling between Pairs of Spins -- Origin of Spin Coupling Interactions -- General Aspects of Spin-Spin Coupling -- Theory of Spin-Spin Coupling -- Correlation of Coupling Constants with Other Physical Properties -- Effect of Exchange -- Spin Decoupling and Double Resonance. |